2,4-Difluoronitrobenzene → HCID 58421662, compound

HRID 406048Notes

Reaction equation

HRID 406048 reaction equation
[C@@H:1]1([OH:8])[CH2:6][CH2:5][CH2:4][CH2:3][C@@H:2]1[OH:7].F[C:10]1[CH:15]=[C:14]([F:16])[CH:13]=[CH:12][C:11]=1[N+:17]([O-:19])=[O:18]>>[F:16][C:14]1[CH:13]=[CH:12][C:11]([N+:17]([O-:19])=[O:18])=[C:10]([CH:15]=1)[O:7][C@H:2]1[CH2:3][CH2:4][CH2:5][CH2:6][C@H:1]1[OH:8]

Participants

3

Reactant 2

HCID 679672,4-DifluoronitrobenzeneHCID 92903rel-(1R,2S)-1,2-Cyclohexanediol

Product 1

HCID 58421662HCID 58421662, compound

Procedure

Prepared analogously to III.1 from cis-1,2-cyclohexandiol (1.0 g) and 0.94 ml 2,4-difluoronitrobenzene.

Sources & evidence

ORD record
ord-1318d7ffbb6c40619c168d7bc27786ce
Source dataset
uspto-grants-2014_06
Patent number
US08754079B2

Reaction notes

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