HuagongsheHuagongshe Chemistry Print Report · For research reference only
Quinoxaline-2-carbaldehyde → 4-Quinoxalin-2-ylmethyl-piperazine-1-carboxylic acid phenylamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Quinoxaline-2-carbaldehyde | HCID 594088 | — |
| Reactant | N-phenylpiperazine-1-carboxamide | HCID 7015289 | — |
| Product | 4-Quinoxalin-2-ylmethyl-piperazine-1-carboxylic acid phenylamide | HCID 57880852 | — |
Reaction Steps
The title compound was prepared from piperazine-1-carboxylic acid phenylamide and 2-quinoxaline-carboxaldehyde in analogy with Example 18. 1H NMR (400 MHz, CDCl3): 8.96 (s, 1H), 8.06-7.98 (m, 2H), 7.72-7.66 (m, 2H), 7.28-7.16 (m, 4H), 7.96-7.92 (m, 1H), 6.42 (s, 1H), 3.85 (s, 2H), 3.48-3.45 (m, 4H), 3.55-3.52 (m, 4H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08530476B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-f90e1c69a8914897820afb4dfe013fbf |
| Source note | uspto-grants-2013_09 |