HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 40634Generated: October 26, 2026
Diisopropylethylamine → HCID 69233532, compound
https://huagongshe.com/reaction/40634
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | (S)-(+)-4-(2,3-Epoxypropoxy)carbazole | HCID 10879208 | — |
| Reactant | Z-(1S,6S)-7-naphthalen-2-yl-7,9-diaza-bicyclo[4.2.2]dec-3-ene | HCID 59686818 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 69233532 | HCID 69233532 | — |
Reaction Steps
(S)-4-Oxiranylmethoxy-9H-carbazole (18.5 mg, 0.077 mmol) and Z-(1S,6S)-7-naphthalen-2-yl-7,9-diaza-bicyclo[4.2.2]dec-3-ene (20 mg, 0.189 mmol) were placed in a μW tube with ethanol (3 ml), DIPEA (15 μL, 0.086 mmol) and heated to 95° C. for 900 sec. The solvent was evaporated and the residue was purified via silica chromatography (30% Ethyl acetate/heptane) to yield the title compound as a residue.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08530475B2 |
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| Source dataset | uspto-grants-2013_09 |
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| ORD ID | ord-e40d41ea9f914e0da5fb86f3c15ab80a |
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| Source note | uspto-grants-2013_09 |
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