HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58102371, compound → HCID 66601032, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58102371 | HCID 58102371 | — |
| Reactant | 4-Bromo-1-cyclopropylpyridin-2(1H)-one | HCID 59635647 | — |
| Product | HCID 66601032 | HCID 66601032 | — |
Reaction Steps
The title compound was prepared from 3-[2,6-dimethyl-4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzyl]-6-(2-hydroxy-2-methyl-propyl)-6-phenyl-[1,3]oxazinan-2-one and 4-bromo-1-cyclopropyl-1H-pyridin-2-one following a procedure analogous to that described in Step 5 of Example 96. LC-MS (Method 5): tR=3.53 min; Mass spectrum (ESI+): m/z=501 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08754076B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-da02cdb69e2e4fec9f2a92a57ee0e020 |
| Source note | uspto-grants-2014_06 |