HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Urea → 2(1H)-Quinazolinone, 4-phenyl-
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Urea | HCID 1176 | — |
| Edukt | 2-Aminobenzophenone | HCID 76080 | — |
| Lösungsmittel | Acetic Acid | HCID 176 | — |
| Produkt | 2(1H)-Quinazolinone, 4-phenyl- | HCID 63430 | — |
Reaktionsschritte
A solution of 2-aminobenzophenone (100 g, 0.51 mol), urea (55 g, 0.93 mol) and acetic acid (300 mL) was stirred at 110° C. for 18 h. The reaction mixture was cooled to rt and filtered. The solid was washed with water and dried under reduced pressure. 4-Phenylquinazolin-2(1H)-one was isolated as a yellow solid and was used without further purification.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08754092B2 |
| Quelldatensatz | uspto-grants-2014_06 |
| ORD ID | ord-fb37e12232134ee796b99af3643c1105 |
| Quellennotiz | uspto-grants-2014_06 |