HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 178483400, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | HCID 178509117 | HCID 178509117 | — |
| Reactant | HCID 178509118 | HCID 178509118 | — |
| Product | HCID 178483400 | HCID 178483400 | — |
Reaction Steps
The title compound (30 mg) was prepared using 185 mg (0.39 mmol) of 4-benzothiazol-2-yl-5-(4-bromobutyl)-2H-pyrazol-3-ylamine, which was derived from 4-(5-amino-4-benzothiazol-2-yl-1H-pyrazol-3-yl)butan-1-ol, and 5 mL of a 2 M solution of methylamine in THF (10 mmol). MS (m/z, ES+): 302.4 (M+1, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08754233B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-92a7b5b44a8a475bbe81f83aef5fea1a |
| Source note | uspto-grants-2014_06 |