HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Iodoaniline → HCID 178462850, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Iodoaniline | HCID 10893 | — |
| Reactant | 2-Phthalimidoethanesulfonyl chloride | HCID 308739 | — |
| Product | HCID 178462850 | HCID 178462850 | — |
Reaction Steps
Prepared according to general method A from 2-phthalimidoethanesulfonyl chloride (1.50 g) and 4-iodoaniline (2.70 g). Yield: 1.56 g (56%). 1H-NMR (CDCl3) δ (ppm) 10.14 (s, 1H), 7.83 (s, 4H), 7.63 (d, J=8.7 Hz, 2H), 7.00 (d, J=8.8 Hz, 2H), 3.94 (t, J=7.1 Hz, 2H), 3.94-3.44 (m, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08530486B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-e1c9c55b1bcd4e9bb9e477498827aec8 |
| Source note | uspto-grants-2013_09 |