HuagongsheHuagongshe Chemistry Print Report · For research reference only
Urea → 5,7-dichloroquinazoline-2,4(1H,3H)-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Urea | HCID 1176 | — |
| Reactant | 4,6-Dichloroanthranilic acid | HCID 290498 | — |
| Product | 5,7-dichloroquinazoline-2,4(1H,3H)-dione | HCID 1508801 | — |
Reaction Steps
Prepared according to general method C from 6-amino-2,4-dichlorobenzoic acid (2.0 g) and urea (5.83 g). Yield 1.72 g (77%) of a solid. 1H-NMR (DMSO-δ6) δ (ppm) 11.39 (br s, 2H), 7.32 (d, J=2.0 Hz, 1H), 7.15 (d, J=2.0 Hz, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08530486B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-ad5cdd3a84b0472f8d5153edea63ef4d |
| Source note | uspto-grants-2013_09 |