HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86684081, compound → HCID 86684082, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86684081 | HCID 86684081 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 86684082 | HCID 86684082 | 81.5% |
Reaction Steps
Following the procedure of Example 151e, and starting with 159a (300 mg, 1.83 mmol) and 10% palladium on carbon (50% wet, 60 mg) afforded 159b as a yellow liquid (200 mg, 81%). 1H NMR (500 MHz, CDCl3) δ 7.24 (s, 1H), 7.14 (t, J=58.5 Hz, 1H), 4.08 (brs, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08754077B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-8b2938618488467b943181e0eb655ed5 |
| Source note | uspto-grants-2014_06 |