HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 408573Generated: October 27, 2026
Methanol → Methyl benzo[d]thiazole-5-carboxylate
https://huagongshe.com/reaction/408573
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 1,3-Benzothiazole-5-carboxylic acid | HCID 2735460 | — |
| Product | Methyl benzo[d]thiazole-5-carboxylate | HCID 22610014 | — |
Reaction Steps
To a suspension of benzothiazole-5-carboxylic acid (1 eq.) in MeOH at 0° C. was added dropwise thionyl chloride (2 eq.). The reaction was stirred at 60° C. for 15 h. The solvents were concentrated under reduced pressure to afford benzothiazole-5-carboxylic acid methyl ester.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08759334B2 |
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| Source dataset | uspto-grants-2014_06 |
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| ORD ID | ord-69a99290ecea4907ad01a632c3befbc3 |
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| Source note | uspto-grants-2014_06 |
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