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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 408670Generated: October 30, 2026

HCID 68727240, compound → HCID 68725336, compound

https://huagongshe.com/reaction/408670

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 68727240HCID 68727240—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
SolventDichloromethaneHCID 6344—
ProductHCID 68725336HCID 68725336—

Reaction Steps

2-Methyl-6-nitro-4-(3-phenylpyrrolidin-1-yl)quinoline (0.29 g; see Preparation 7 above) and palladium on carbon (10%, 0.2 g) in ethanol (10 mL) and dichloromethane (4 mL) was stirred under a hydrogen atmosphere for 3 hours. The reaction mixture was filtered and concentrated to give the title compound as a thick yellow oil, which was used without further purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08759348B2
Source datasetuspto-grants-2014_06
ORD IDord-f8326fbf00ba4e609921a44af54e8e5b
Source noteuspto-grants-2014_06