HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57877112, compound → HCID 57500708, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57877112 | HCID 57877112 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 57500708 | HCID 57500708 | — |
Reaction Steps
A suspension of 1-[2-(3-fluoro-4-nitro-phenoxy)-ethyl]-pyrrolidine (1.96 g, 7.7 mmol) and 10% palladium on carbon (0.2 g) in MeOH (40 mL) is stirred for 0.5 h at RT, under a hydrogen atmosphere. The reaction mixture is filtered through a pad of celite and concentrated to provide the title compound. ESI-MS: 225.1 [MH]+; tR=0.95 min (system 1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08759517B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-e8d8c8adcea64d8891f690866d1f629c |
| Source note | uspto-grants-2014_06 |