HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-(methylamino)-3-nitrobenzoate → Methyl 3-amino-4-(methylamino)benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-(methylamino)-3-nitrobenzoate | HCID 7650848 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | Methyl 3-amino-4-(methylamino)benzoate | HCID 15586064 | 96.1% |
Reaction Steps
3-amino-4-methylamino-benzoic acid methyl ester (677 mg) was prepared by following General Procedure B starting from 4-methylamino-3-nitro-benzoic acid methyl ester (822 mg) and Pd/C (10% by weight, 82 mg). The crude product was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08759535B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-c0c7b5facc1644408fce75264afc20cd |
| Source note | uspto-grants-2014_06 |