HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylamine → Methyl 4-(ethylamino)-3-nitrobenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylamine | HCID 6341 | — |
| Reactant | Methyl 4-chloro-3-nitrobenzoate | HCID 735797 | — |
| Product | Methyl 4-(ethylamino)-3-nitrobenzoate | HCID 20626654 | — |
Reaction Steps
4-Ethylamino-3-nitro-benzoic acid methyl ester (4.0 g) was prepared by following General Procedure A starting from methyl 4-chloro-3-nitrobenzoate (5.0 g) in ethylamine (2.0 M in THF, 50 mL). The crude product was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08759535B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-a3a1c21ff16f4d7c9e6cc1b5dd465180 |
| Source note | uspto-grants-2014_06 |