HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropylamine → HCID 2823414, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropylamine | HCID 6363 | — |
| Reactant | Methyl 4-chloro-3-nitrobenzoate | HCID 735797 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 2823414 | HCID 2823414 | 81.4% |
Reaction Steps
4-Isopropylamino-3-nitro-benzoic acid methyl ester (900.0 mg) was prepared by following General Procedure A starting from methyl 4-chloro-3-nitrobenzoate (1.0 g) and isopropyl amine (325.0 mg) in DMF (10.0 mL). The crude product was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08759535B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-8f010a7b136444e9808941c15219e80c |
| Source note | uspto-grants-2014_06 |