HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-BOC-ethylenediamine → HCID 67332341, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-BOC-ethylenediamine | HCID 187201 | — |
| Reactant | Methyl 4-chloro-3-nitrobenzoate | HCID 735797 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 67332341 | HCID 67332341 | 76.2% |
Reaction Steps
4-(2-tert-Butoxycarbonylamino-ethylamino)-3-nitro-benzoic acid methyl ester (650.0 mg) was prepared by following General Procedure A starting from methyl 4-chloro-3-nitrobenzoate (542.0 mg) and (2-amino-ethyl)-carbamic acid tert-butyl ester (500.0 mg) in DMF (3.0 mL). The crude product was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08759535B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-454a9aafd45543a6a4351ff9f206f737 |
| Source note | uspto-grants-2014_06 |