HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Azide → 1-Azido-2-(2-methoxyethoxy)ethane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | 1-Bromo-3,6-dioxaheptane | HCID 123532 | — |
| Product | 1-Azido-2-(2-methoxyethoxy)ethane | HCID 10034751 | 76.5% |
Reaction Steps
1-Azido-2-(2-methoxy-ethoxy)-ethane (607 mg) was prepared by following General Procedure U starting from 1-bromo-2-(2-methoxy-ethoxy)-ethane (1.0 g) and sodium azide (1.07 g). The crude product was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08759535B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-da46aa2df9f94867b4ddaed513066231 |
| Source note | uspto-grants-2014_06 |