HuagongsheHuagongshe Chemistry Print Report · For research reference only
[2-(2-Dibenzylamino-ethoxy)-ethyl]methyl-carbamic acid tert-butyl ester → tert-butyl N-(2-(2-aminoethoxy)ethyl)-N-methylcarbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | [2-(2-Dibenzylamino-ethoxy)-ethyl]methyl-carbamic acid tert-butyl ester | HCID 67332450 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | tert-butyl N-(2-(2-aminoethoxy)ethyl)-N-methylcarbamate | HCID 85823338 | 91.3% |
Reaction Steps
[2-(2-Amino-ethoxy)-ethyl]-methyl-carbamic acid tert-butyl ester (100 mg) was prepared following General Procedure T starting from [2-(2-dibenzylamino-ethoxy)-ethyl]-methyl-carbamic acid tert-butyl ester (200 mg) and Pd—C (40 mg) in methanol (1.5 mL).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08759535B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-3bcd6dd6aaa54ab5aa47ded7783c635f |
| Source note | uspto-grants-2014_06 |