HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
N-(2-Chloroethyl)dibenzylamine → [2-(2-Dibenzylamino-ethoxy)-ethyl]dimethyl-amine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | N-(2-Chloroethyl)dibenzylamine | HCID 5820 | — |
| Edukt | 2-(Dimethylamino)ethanol | HCID 7902 | — |
| Edukt | Potassium Hydroxide | HCID 14797 | — |
| Katalysator | Tetrabutylammonium Bromide | HCID 74236 | — |
| Lösungsmittel | 1,4-Dioxane | HCID 31275 | — |
| Produkt | [2-(2-Dibenzylamino-ethoxy)-ethyl]dimethyl-amine | HCID 67332185 | — |
Reaktionsschritte
[2-(2-Dibenzylamino-ethoxy)-ethyl]-dimethyl-amine was prepared following General Procedure S starting from dibenzyl-(2-chloro-ethyl)-amine (640 mg), 2-dimethylamino-ethanol (325 mg), 50% (w/w) KOH solution (3 mL) and tetrabutylammonium bromide (95 mg) in dioxane (3 mL).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08759535B2 |
| Quelldatensatz | uspto-grants-2014_06 |
| ORD ID | ord-4ae372d5b90a419eb5e8acf22be3a170 |
| Quellennotiz | uspto-grants-2014_06 |