HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Dimethylcarbamoylmethyl-4-methylamino-3-nitro-benzamide → 3-Amino-N-dimethylcarbamoylmethyl-4-methylamino-benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Dimethylcarbamoylmethyl-4-methylamino-3-nitro-benzamide | HCID 9303598 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 3-Amino-N-dimethylcarbamoylmethyl-4-methylamino-benzamide | HCID 67333499 | 98% |
Reaction Steps
3-Amino-N-dimethylcarbamoylmethyl-4-methylamino-benzamide (700 mg) was prepared by following General Procedure B starting from N-dimethylcarbamoylmethyl-4-methylamino-3-nitro-benzamide (800 mg) and Pd—C (160 mg) in methanol (10 mL).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08759535B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-d890142553bc4e598c7639be7b6c4c30 |
| Source note | uspto-grants-2014_06 |