1,2,4-Trimethylcyclohex-3-ene-1-carbaldehyde → HCID 11469653, compound
Reaction equation
[CH3:1][C:2]1([CH:10]=[O:11])[CH2:7][CH2:6][C:5]([CH3:8])=[CH:4][CH:3]1[CH3:9].[CH:12]([Mg]Br)([CH3:14])[CH3:13]>>[CH3:13][CH:12]([CH3:14])[CH:10]([C:2]1([CH3:1])[CH2:7][CH2:6][C:5]([CH3:8])=[CH:4][CH:3]1[CH3:9])[OH:11]Participants
3
Procedure
2-methyl-1-(1,2,4-trimethyl-3-cyclohexen-1-yl)-1-propanol (compound 1) was prepared from 1,2,4-trimethyl-3-cyclohexene-1-carboxaldehyde and isopropylmagnesium bromide (reaction 1 above).
Sources & evidence
- ORD record
- ord-9f65cf95e7a24ced861ad2b972ddffac
- Source dataset
- uspto-grants-2003_05
- Patent number
- US06559118B1
Reaction notes
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