HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzeneacetic acid, 3,5-difluoro-α-hydroxy-, (αS)- → HCID 131723829, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzeneacetic acid, 3,5-difluoro-α-hydroxy-, (αS)- | HCID 6951479 | — |
| Reactant | HCID 23552795 | HCID 23552795 | — |
| Product | HCID 131723829 | HCID 131723829 | — |
Reaction Steps
Following General Procedure D and using (S)-3,5-difluoromandelic acid (Example L) and 5-(L-valinyl)-amino-10-fluoro-7-methyl-5,7-dihydro-6H-dibenz[b,d]azepin-6-one hydrochloride (Example 7-W), the title compound was prepared. The product was purified by chromatography (silica, 2.5% MeOH/CHCl3).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06559141B2 |
| Source dataset | uspto-grants-2003_05 |
| ORD ID | ord-04d6edc0a7a74de4addf1c5385676255 |
| Source note | uspto-grants-2003_05 |