化工社化工社 化学情報印刷レポート · 研究参考用
3,4-Dichloroaniline → Ethyl N-(3,4-dichlorophenyl)alaninate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3,4-Dichloroaniline | HCID 7257 | — |
| 反応物 | Ethyl pyruvate | HCID 12041 | — |
| 生成物 | Ethyl N-(3,4-dichlorophenyl)alaninate | HCID 169545 | — |
反応手順
Following General Procedure AA above and using 3,4-dichloroaniline (Aldrich) and ethyl pyruvate (Aldrich), the title compound was prepared as an oil. The reaction was monitored by tlc on silica gel (Rf=0.4 in 25% EtOAc/hexanes) and purification was by preparative plate chromatography (silica gel using 25% EtOAc/hexanes as the eluant).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06559141B2 |
| 出典データセット | uspto-grants-2003_05 |
| ORD ID | ord-7235e339910648328db529b8ed989bb6 |
| 出典メモ | uspto-grants-2003_05 |