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2-Naphthylamine → N-(2-naphthyl)alanine Methyl Ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Naphthylamine | HCID 7057 | — |
| 反応物 | Methyl pyruvate | HCID 11748 | — |
| 生成物 | N-(2-naphthyl)alanine Methyl Ester | HCID 22876174 | — |
反応手順
Following reductive amination General Procedure AA above and using 2-aminonaphthalene (Aldrich) and methyl pyruvate (Aldrich), the title compound was prepared. The reaction was monitored by silica gel tlc (Rf=0.50 in 25% EtOAc/hexanes). Purification was by flash chromatography with silica gel using 25% EtOAc/hexanes as the eluant.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06559141B2 |
| 出典データセット | uspto-grants-2003_05 |
| ORD ID | ord-1fee59f615c240c1a34f52d053be4d77 |
| 出典メモ | uspto-grants-2003_05 |