N,N-Dimethylbenzylamine → HCID 18541161, compound

Participants

Reaction Steps

N,N-Dimethyl benzylamine (7 ml) was dissolved in 40 ml of dichloromethane and chlorosulfonic acid (12 ml) was slowly added at 0° C. The reaction mixture was stirred at room temperature for 4 hours. The reaction mixture was poured into ice to give solids, which was collected by filtration. 2.63 g of the titled compound was obtained. Additional crops (1.34 g) was obtained from the dichloromethane extraction of the filtrate.

Provenance & Evidence