Sodium Cyanide → HCID 69556631, compound

Participants

Reaction Steps

In a manner analogous to Preparation 1, 3,4-dichlorobenzaldehyde (0.56 g, 3.20 mmol), tosylmethylisocyanide (0.75 g, 3.84 mmol) and NaCN (0.02 g, 0.40 mmol) gave the desired compound as a tan solid. 1H NMR (300 MHz, CDCl3) δ 7.85 (d, J=8.3 Hz, 2H), 7.50 (d, J=8.3 Hz, 1H), 7.35 (m, 3H), 7.15 (m, 2H), 6.00 (d, J=6.2 Hz. 1H), 4.96 (dd, J=6.2, 1.7 Hz, 1H), 2.47 (s, 3H).

Provenance & Evidence