HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperonal → HCID 12116612, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperonal | HCID 8438 | — |
| Reactant | Sodium Cyanide | HCID 8929 | — |
| Reactant | Tosylmethyl isocyanide | HCID 161915 | — |
| Product | HCID 12116612 | HCID 12116612 | — |
Reaction Steps
In a manner analogous to Preparation 1, tosylmethylisocyanide (0.23 g, 1.20 mmol), piperonal (0.19 g, 1.26 mmol) and NaCN (5.9 mg, 0.12 mmol) gave the desired compound as a tan solid. MS(ES+) m/z 346.5 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06559172B1 |
| Source dataset | uspto-grants-2003_05 |
| ORD ID | ord-e361ace01c8b4b8badc8189b9b9a1c40 |
| Source note | uspto-grants-2003_05 |