HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Cyanide → HCID 54117280, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Cyanide | HCID 8929 | — |
| Reactant | Tosylmethyl isocyanide | HCID 161915 | — |
| Reactant | 4-Chloro-3-Fluorobenzaldehyde | HCID 2724985 | — |
| Product | HCID 54117280 | HCID 54117280 | — |
Reaction Steps
In a manner analogous to Preparation 1, tosylmethylisocyanide (0.30 g, 1.52 mmol), 4-chloro-3-fluorobenzaldehyde (0.25 g, 1.60 mmol) and NaCN (10 mg, 0.20 mmol) gave the desired compound as a tan solid. MS(ES+) m/z 373.5 (M+Na+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06559172B1 |
| Source dataset | uspto-grants-2003_05 |
| ORD ID | ord-75ab6e89245a41b6afcbc9f3d5a0c8c3 |
| Source note | uspto-grants-2003_05 |