HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetate → HCID 178468162, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | HCID 178468164 | HCID 178468164 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178468162 | HCID 178468162 | 95% |
Reaction Steps
A 500 mL Parr bottle was charged with 400 mg Pd(OH)2, 7.0 g (24.1 mmol) trans-(−)-[4-(1-hydroxy-ethyl)-cyclohexylmethyl]-carbamic acid benzyl ester, 125 mL ethyl acetate and 125 ml MeOH. The bottle was placed under 50 psi H2 and shaken for 2 hours. The suspension was then filtered through Celite and concentrated to give 3.6 g of a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06559168B2 |
| Source dataset | uspto-grants-2003_05 |
| ORD ID | ord-b2c33bbb57e24642becf9eee8745981d |
| Source note | uspto-grants-2003_05 |