HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 411763Generated: October 26, 2026
Calcium chloride, dihydrate → Calcium bicyclo(2.2.1)heptane-2,3-dicarboxylate
https://huagongshe.com/reaction/411763
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Calcium chloride, dihydrate | HCID 6093260 | — |
| Reactant | bicyclo2.2.1heptane-2,3-dicarboxylic acid, disodium salt | HCID 21981355 | — |
| Solvent | Water | HCID 962 | — |
| Product | Calcium bicyclo(2.2.1)heptane-2,3-dicarboxylate | HCID 21981350 | — |
Reaction Steps
To a solution of disodium bicyclo[2.2.1]heptane-2,3-dicarboxylate (22.6 g, 0.1 mol) in water (150 g) was added a solution of calcium chloride dihydrate (14.7 g, 0.1 mol) in water (100 g). The mixture stirred at 60° C. for 2 hours. The resulting white precipitate was filtered. The white powdery product was dried and milled (m.p. >300° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06559211B2 |
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| Source dataset | uspto-grants-2003_05 |
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| ORD ID | ord-45a11144c85a4e5e82113832017c3fbd |
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| Source note | uspto-grants-2003_05 |
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