Sulfuric Acid → 6-Chlorohexanoic acid

HRID 411796Notes

Reaction equation

HRID 411796 reaction equation
[C:1]([OH:8])(=[O:7])[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6].S(=O)(=O)(O)O.[Cl:14]Cl>>[Cl:14][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2][C:1]([OH:8])=[O:7]

Participants

4

Reactant 3

HCID 1118Sulfuric AcidHCID 8892Hexanoic AcidHCID 24526Chlorine

Product 1

HCID 202096-Chlorohexanoic acid

Procedure

147 parts by mass of the caproic acid were added to 1,000 parts by mass of 27N sulfuric acid saturated with chlorine and were reacted for 6 hours at 25° C. to obtain 95 parts by mass of 6-chlorocaproic acid.

Workup

  1. customwere reacted for 6 hours at 25° C.

Sources & evidence

ORD record
ord-f2882aa9cad04919ac8b08b0b5d0bd19
Source dataset
uspto-grants-2003_05
Patent number
US06559275B2

Reaction notes

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