HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Tetrahydrothiazine-3-one → 4-Benzylthiomorpholin-3-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Tetrahydrothiazine-3-one | HCID 88402 | — |
| Reactant | 4-(Bromomethyl)-1,2-dichlorobenzene | HCID 639726 | — |
| Reactant | 4-(3,4-Dichlorobenzyl)-thiomorpholin-3-one | HCID 12083011 | — |
| Product | 4-Benzylthiomorpholin-3-one | HCID 14941172 | — |
Reaction Steps
In the same manner, 4-(3,4-dichlorobenzyl)-thiomorpholin-3-one was prepared in 89% yield from 3,4-dichlorobenzyl bromide and thiomorpholin-3-one as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06562813B2 |
| Source dataset | uspto-grants-2003_05 |
| ORD ID | ord-d12fb8c7dd2a482b9551ddcb7e9bccb7 |
| Source note | uspto-grants-2003_05 |