HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 18534817, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethylene Oxide | HCID 6354 | — |
| Reactant | 3,3,5,5-Tetramethylmorpholin-2-one | HCID 13131203 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18534817 | HCID 18534817 | — |
Reaction Steps
45.0 g (0.29 moles) of 3,3,5,5-tetramethyl-2-morpholone are dissolved in 450 ml of methanol. The solution is poured into an autoclave, added with 1 ml of concentrated HCl (37%) (% w/w) and pressurized with ethylene oxide (2 bars).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06562815B1 |
| Source dataset | uspto-grants-2003_05 |
| ORD ID | ord-b4fab4f1dc19467d93f8f806b6845953 |
| Source note | uspto-grants-2003_05 |