2-Amino-3-methylbenzamide → 3-Methyl-2-(2-n-propoxybenzamido)benzamide

HRID 412038Notes

Reaction equation

HRID 412038 reaction equation
[NH2:1][C:2]1[C:10]([CH3:11])=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([NH2:6])=[O:5].[CH2:12]([O:15][C:16]1[CH:24]=[CH:23][CH:22]=[CH:21][C:17]=1[C:18](Cl)=[O:19])[CH2:13][CH3:14]>>[CH3:11][C:10]1[C:2]([NH:1][C:18](=[O:19])[C:17]2[CH:21]=[CH:22][CH:23]=[CH:24][C:16]=2[O:15][CH2:12][CH2:13][CH3:14])=[C:3]([CH:7]=[CH:8][CH:9]=1)[C:4]([NH2:6])=[O:5]

Participants

3

Reactant 2

HCID 142218072-Amino-3-methylbenzamideHCID 159219132-Propoxybenzoyl chloride

Product 1

HCID 185366023-Methyl-2-(2-n-propoxybenzamido)benzamide

Procedure

The title compound was prepared from 2-amino-3-methylbenzamide and 2-n-propoxybenzoyl chloride following the procedure of Preparation 5 and was obtained as a colourless solid (71%), m.p. 140-142° C.

Workup

  1. customthe procedure of Preparation 5

Sources & evidence

ORD record
ord-45bf2ac6b30948aaae334efa24246988
Source dataset
uspto-grants-2003_05
Patent number
US06562830B1

Reaction notes

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