HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → Methyl 3-(benzyloxy)-5-methoxybenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | Methyl 3,5-Dihydroxybenzoate | HCID 75076 | — |
| Product | Methyl 3-(benzyloxy)-5-methoxybenzoate | HCID 12658782 | — |
Reaction Steps
Following the procedure of Example 80(a) except substituting methyl 3-hydroxy-5-methoxybenzoate for methyl 3,5-dihydroxybenzoate and benzyl bromide for iodomethane, the title compound was prepared as a tan oil (1.2 g, 4.4 mmol). 1H NMR (400 MHz, CDCl3) δ 7.45-7.31 (m, 6H), 7.24 (s, 1H), 6.76 (m, 1H), 5.09 (s, 2H), 3.95 (s, 3H), 3.84 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06562842B2 |
| Source dataset | uspto-grants-2003_05 |
| ORD ID | ord-9e2814c6b9de4becace378750f86b4ee |
| Source note | uspto-grants-2003_05 |