4-Methoxybenzenesulfonyl chloride → HCID 18538668, compound

HRID 412947Notes

Reaction equation

HRID 412947 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([N:9]([CH2:22][CH2:23][CH2:24][N:25]2[CH2:30][CH2:29][CH:28]([NH:31][CH3:32])[CH2:27][CH2:26]2)[C:10]([CH:12]2[CH2:17][CH2:16][N:15]([S:18]([CH3:21])(=[O:20])=[O:19])[CH2:14][CH2:13]2)=[O:11])[CH:5]=[CH:6][C:7]=1[Cl:8].[CH3:33][O:34][C:35]1[CH:40]=[CH:39][C:38]([S:41](Cl)(=[O:43])=[O:42])=[CH:37][CH:36]=1>>[Cl:1][C:2]1[CH:3]=[C:4]([N:9]([CH2:22][CH2:23][CH2:24][N:25]2[CH2:26][CH2:27][CH:28]([N:31]([S:41]([C:38]3[CH:37]=[CH:36][C:35]([O:34][CH3:33])=[CH:40][CH:39]=3)(=[O:43])=[O:42])[CH3:32])[CH2:29][CH2:30]2)[C:10]([CH:12]2[CH2:13][CH2:14][N:15]([S:18]([CH3:21])(=[O:19])=[O:20])[CH2:16][CH2:17]2)=[O:11])[CH:5]=[CH:6][C:7]=1[Cl:8]

Participants

3

Reactant 2

HCID 74014-Methoxybenzenesulfonyl chlorideHCID 18538881HCID 18538881, compound

Product 1

HCID 18538668HCID 18538668, compoundYield 87%

Procedure

The title compound was prepared using a similar procedure to that described for example 195 from the title compound of example 323 and 4-methoxybenzenesulfonyl chloride, yield 87%.

Sources & evidence

ORD record
ord-123347e12d0a42adb6b1dc99c6856dca
Source dataset
uspto-grants-2003_05
Patent number
US06562978B1

Reaction notes

Loading…