Bromine → HCID 11265458, compound

Participants

Reaction Conditions

Reaction Steps

Bromine (28.8 g, 0.18 mol) (dissolved in dioxane (500 ml)) was added dropwise to a solution of 2-methoxy-6-methylsulfanylbenzaldehyde (22 g, 0.12 mol) in dioxane (500 ml), and the mixture was stirred at 50° C. for 6 h. The mixture was then concentrated, the residue was taken up in CH2Cl2 and the mixture was washed with water, dried over MgSO4 and concentrated. The solid was recrystallized from diisopropyl ether.

Provenance & Evidence