HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 135856766, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 2-[2-Ethoxy-5-[(4-methyl-1-piperazinyl)sulfonyl]phenyl]-5-ethyl-7-propylimidazo[5,1-f][1,2,4]triazin-4(1H)-one | HCID 135544159 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 135856766 | HCID 135856766 | — |
Reaction Steps
300 mg (0.61 mmol) of 2-[2-ethoxy-5-(4-methyl-piperazine-1-sulphonyl)-phenyl]-5-ethyl-7-propyl-3H-imidazo[5,1-f][1,2,4]triazin-4-one are dissolved in a mixture of ether and dichloromethane and admixed with 2 ml of a 1M solution of HCl in ether. After 20 minutes, the precipitated solid is filtered off with suction and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06566360B1 |
| Source dataset | uspto-grants-2003_05 |
| ORD ID | ord-5ed3ad38094a419ab3d8958a6afc8bbc |
| Source note | uspto-grants-2003_05 |