HRID413127

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID3595059

5-Bromothiophene-2-carbonitrile

C5H2BrNS

HCID10987806

(4,4-Dimethyl-2-oxo-1,4-dihydro-2H-3,1-benzoxazin-6-yl)boronic acid

C10H12BNO4

PRODUCTS

生成物

结构：CC1(C)OC(=O)Nc2ccc(-c3ccc(C#N)s3)cc21

HCID9878929

未命名化合物

PROCEDURE

实验过程

Prepared according to Procedure B from 5-bromo-2-thiophenecarbonitrile and (1,4-dihydro-4,4-dimethyl-2-oxo-2H-3,1-benzoxazin-6-yl)boronic acid. Off-white solid: mp 264-266° C. 1H-NMR (DMSO-d6) δ10.3 (s, 1H), 7.97 (d, 1H, J=7.9 Hz), 7.60-7.66 (m, 3H). 6.96 (d, 1H, J=8.1 Hz), 1.65 (S, 6H). MS (APCI) m/z 285 (M+H)+, 302 (M+NH4)+. Anal. Calc. For C15H12N2O2S: C, 63.36; H, 4.25; N, 9.85. Found: C, 63.01; H, 4.36; N, 9.39.

WORKUP

后处理

customPrepared