Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethylamine → 4-hydroxy-N,N-dimethyl-4-phenyl-butyramide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethylamine | HCID 674 | — |
| 반응물 | gamma-Phenyl-gamma-butyrolactone | HCID 13884 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | 4-hydroxy-N,N-dimethyl-4-phenyl-butyramide | HCID 13000819 | — |
반응 단계
A solution of γ-phenyl-γ-butyrolactone (4.84 g, 29.8 mmol) in 200 ml of a 2 molar solution of dimethylamine in THF was stirred under a nitrogen atmosphere at room temperature for 2 days. The solvent was removed under reduced pressure to give 6.26 g of 4-hydroxy-N,N-dimethyl-4-phenyl-butyramide as a light brown oil, MS [M+H]+ m/e 208.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06566375B1 |
| 출처 데이터셋 | uspto-grants-2003_05 |
| ORD ID | ord-8be19e4529674ff490614627af3e8b0f |
| 출처 메모 | uspto-grants-2003_05 |