HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(2-nitro-4-trifluoromethylsulfonyl-phenyl)-acetamide → 2-Nitro-4-(trifluoromethanesulfonyl)aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(2-nitro-4-trifluoromethylsulfonyl-phenyl)-acetamide | HCID 22325341 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | Water | HCID 962 | — |
| Product | 2-Nitro-4-(trifluoromethanesulfonyl)aniline | HCID 4529469 | — |
Reaction Steps
Reflux N-(2-nitro-4-trifluoromethylsulfonyl-phenyl)-acetamide (600 mg) for 40 minutes in concentrated HCl (15 mL) and water (5 mL). Cool the mixture to room temperature and collect the precipitate obtain 2-nitro-4-trifluoromethylsulfonyl-phenylamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06566367B2 |
| Source dataset | uspto-grants-2003_05 |
| ORD ID | ord-d03c03ad5a114f54b7c8338afc47931b |
| Source note | uspto-grants-2003_05 |