HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → N,N-Bis(2-chloroethyl)-N'-phenylcarbamimidic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 22390756 | HCID 22390756 | — |
| Product | N,N-Bis(2-chloroethyl)-N'-phenylcarbamimidic acid | HCID 247712 | — |
Reaction Steps
26.44 ml of thionyl chloride are added, at 0° C., to a solution of 0.173 mol of the product obtained in Step 1 in 100 ml of dichloromethane. After reacting for 4 hours at reflux and then for 12 hours at ambient temperature, the reaction mixture is concentrated under reduced pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06566364B2 |
| Source dataset | uspto-grants-2003_05 |
| ORD ID | ord-7795bb81d61a4f37b1b3c8f85dca6f17 |
| Source note | uspto-grants-2003_05 |