HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2-Hydroxyethyl)piperazine → HCID 18523542, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2-Hydroxyethyl)piperazine | HCID 7677 | — |
| Reactant | Sodium triacetoxyborohydride | HCID 5049666 | — |
| Reactant | HCID 9912542 | HCID 9912542 | — |
| Catalyst | Acetic Acid | HCID 176 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 18523542 | HCID 18523542 | — |
Reaction Steps
The product of Example 15 (0.001 g) was dissolved in N,N-dimethylformamide (0.2 ml), N-(2-hydroxyethyl)piperazine (0.0008 g) and 1 drop of acetic acid were added. After 1 hour a solution of sodium triacetoxyborohydride (0.0013 g) in N,N-dimethylformamide (0.1 ml) was added and the solution shaken at room temperature for 24 hours. The solvent was removed to give the product as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06566376B1 |
| Source dataset | uspto-grants-2003_05 |
| ORD ID | ord-dfaa6df7011f4a5ebef93c2028eebdbc |
| Source note | uspto-grants-2003_05 |