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HRID413322

反应详情

EQUATION

反应方程式

HRID 413322 的结构方程式

REACTANTS

反应物

2
结构：CC=CC(=O)CC
HCID17244

4-Hexen-3-one

C6H10O

结构：CC1=NN(c2ccc3[nH]c(=O)cc(C(F)(F)F)c3c2)CC1
HCID67156328

6-(4,5-Dihydro-3-methyl-1H-pyrazol-1-yl)-4-(trifluoromethyl)-2(1H)-quinolinone

C14H12F3N3O

PRODUCTS

生成物

1
结构：CCC1=NN(c2ccc3[nH]c(=O)cc(C(F)(F)F)c3c2)C(C)C1
HCID67156931

未命名化合物

PROCEDURE

实验过程

This compound was prepared from the condensation of Compound 793 (Structure 159 of Scheme XXXIII) and 2-hexen-4-one as yellow solid. 1H NMR (500 MHz, DMSO-d6) 12.1 (bs, 1H), 7.41 (dd, J=8.8, 2.4, 1H), 7.34 (d, J=8.8, 1H), 7.21 (bs, 1H), 6.92 (s, 1H), 4.37-4.28 (m, 1H), 3.12 (dd, J=17.1, 10.2, 1H), 2.53 (dd, J=17.1, 4.9, 1H), 2.37 (q, J=7.3, 2H), 1.12 (t, J=7.3, 3H), 1.12 (d, J=5.9, 3H).