Sodium Azide → HCID 12971695, compound

Participants

Reaction Steps

6-Methyl-3-(toluene-4-sulfonyl)-3H-benzo[1,2,3]oxathiazole 2,2-dioxide (100 mg, 0.295 mmol) is dissolved in acetonitrile (5 ml). A solution of sodium azide (of 20 mg, 0.29 mmol of sodium azide in 1 ml of H2O) is added to this solution, and the mixture is stirred at RT overnight. The mixture is then stirred at 60° C. for 1 h, the solvent is distilled off under reduced pressure and the residue is purified by RP chromatography.

Provenance & Evidence