HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 14255313, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 2-Phenoxyphenylacetic acid | HCID 141222 | — |
| Product | HCID 14255313 | HCID 14255313 | 91% |
Reaction Steps
A solution of 2-phenoxyphenylacetic acid (2.75 g) in dry methanol (30 ml) containing concentrated sulphuric acid (0.3 ml) was heated under reflux for 2 hours then allowed to cool, poured into water and extracted with ether. The extracts were washed with water, dried and concentrated under reduced pressure to give methyl 2-phenoxyphenylacetate (2.65 g, 91%) as a pale yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06566547B1 |
| Source dataset | uspto-grants-2003_05 |
| ORD ID | ord-267c273c552f407492c7a6c287219f6b |
| Source note | uspto-grants-2003_05 |