化工社化工社 化学情報印刷レポート · 研究参考用
2,3-Dichlorobenzaldehyde → Ethyl 4-(2-chloro-6-formylphenylthio)butyrate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2,3-Dichlorobenzaldehyde | HCID 35745 | — |
| 反応物 | Ethyl 4-sulfanylbutanoate | HCID 271824 | — |
| 生成物 | Ethyl 4-(2-chloro-6-formylphenylthio)butyrate | HCID 11471721 | — |
反応手順
Ethyl 4-(2-chloro-6-formylphenylthio)butyrate was synthesized from 2,3-dichlorobenzaldehyde and ethyl 4-mercaptobutyrate in the same manner as Example 2. After column chromatography, vacuum concentration yielded ethyl 4-(2-chloro-6-formylpehylthio)butyrate (Yield 70%) as a yellow oily matter.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06566535B1 |
| 出典データセット | uspto-grants-2003_05 |
| ORD ID | ord-475a4ea6c3a14d18bc0949ac7807b9ae |
| 出典メモ | uspto-grants-2003_05 |