HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-n-Octadecyloxybenzoic acid → 4-(trans-2-Decenyloxy)-benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-n-Octadecyloxybenzoic acid | HCID 139993 | — |
| Reactant | Lithium hydroxide, monohydrate | HCID 168937 | — |
| Reactant | Methyl-4-(trans-2-decenyloxy)-benzoate | HCID 18521070 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 4-(trans-2-Decenyloxy)-benzoic acid | HCID 18521013 | — |
Reaction Steps
The ester 35g 565 mg, 1.95 mmol), and lithium hydroxide monohydrate (817 mg, 19.5 mmol) in 20 ml methanol were reacted according to the procedure for compound 36a. The yield was 482 mg (89% of a white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06569504B1 |
| Source dataset | uspto-grants-2003_05 |
| ORD ID | ord-ccede109ff2a4b66956b2756cfc70ce9 |
| Source note | uspto-grants-2003_05 |