huagongshe.com
HRID413770

反应详情

EQUATION

反应方程式

HRID 413770 的结构方程式

REACTANTS

反应物

3
结构：c1ccncc1
HCID1049

Pyridine

C5H5N

结构：CCOC(=O)C(C(C)=O)C(C)=O
HCID79063

Ethyl 2-acetylacetoacetate

C8H12O4

结构：Cl.NNc1cccc(F)c1
HCID2723914

(3-Fluorophenyl)hydrazine--hydrogen chloride (1/1)

C6H8ClFN2

PRODUCTS

生成物

1
结构：CCOC(=O)c1c(C)nn(-c2cccc(F)c2)c1C
HCID9856538

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

Similar to Example 1, equimolar amounts of 3-fluorophenylhydrazine hydrochloride and 2-acetyl-3-oxo-butyric acid ethyl ester were combined in a solution of 50% pyridine in ethanol. Analysis showed that resulting solid was the named product (m.p. 55° C.-56.1° C.).

WORKUP

后处理

  1. customthat resulting solid