HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 413794Generated: October 29, 2026
Potassium Carbonate → HCID 18522117, compound
https://huagongshe.com/reaction/413794
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-(Bromomethyl)-1,2-dichlorobenzene | HCID 639726 | — |
| Reactant | HCID 18522118 | HCID 18522118 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 18522117 | HCID 18522117 | — |
Reaction Steps
3,4-Dichlorobenzyl bromide (1.02 g) was added to a stirred solution of methyl 4-acetoxy-5-methoxyindole-2-carboxylate (0.8 g) and potassium carbonate (0.97 g) in acetonitrile (30 ml) under an atmosphere of argon. The reaction was heated at 80° C. for 16 hours, then concentrated in vacuo and the residue partitioned between ethyl acetate and water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06569888B1 |
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| Source dataset | uspto-grants-2003_05 |
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| ORD ID | ord-f65082adba8748de9b8a52b871c1bba5 |
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| Source note | uspto-grants-2003_05 |
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